Chemical characterization of tequila maturation process and their connection with the physicochemical properties of the cask
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The effect of time in the maturation process of Tequila employing two types of casks was studied: A new (labeled as Cask-New) and a medium-toasted cask (15 min at 200 °C) (labeled as Cask-MT). For that purpose, the wood used in the casks was characterized physicochemically, and its properties were contrasted with the physicochemical characterization of the beverage throughout the maturation time. To understand the kinetic maturation process, mathematical models were used. The best model that represented the polyphenol (I280) and flavonoid (I365) extraction was proposed by Minchev %26amp; Minkov. The extraction rate constants were: kcask-new,I280 = 0.233 month−1 vs. kCask-MT,I280 = 0.560 month−1, and kcask-new,I365 = 0.132 month-1 vs. kCask-MT,I365 = 0.383 month−1, explaining that the extraction process is slower in Cask-MT due to textural characteristics of casks, mainly related to the thermic treatment used in the toasting stage, which collapses the mesoporous structure having mass transfer limitations. The results obtained allow a better description of the maturation process, a fundamental step from a food engineering standpoint. The next step in the research should be to validate the proposed model to improve the final product quality. © 2021 Elsevier Inc.
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The effect of time in the maturation process of Tequila employing two types of casks was studied: A new (labeled as Cask-New) and a medium-toasted cask (15 min at 200 °C) (labeled as Cask-MT). For that purpose, the wood used in the casks was characterized physicochemically, and its properties were contrasted with the physicochemical characterization of the beverage throughout the maturation time. To understand the kinetic maturation process, mathematical models were used. The best model that represented the polyphenol (I280) and flavonoid (I365) extraction was proposed by Minchev & Minkov. The extraction rate constants were: kcask-new,I280 = 0.233 month−1 vs. kCask-MT,I280 = 0.560 month−1, and kcask-new,I365 = 0.132 month-1 vs. kCask-MT,I365 = 0.383 month−1, explaining that the extraction process is slower in Cask-MT due to textural characteristics of casks, mainly related to the thermic treatment used in the toasting stage, which collapses the mesoporous structure having mass transfer limitations. The results obtained allow a better description of the maturation process, a fundamental step from a food engineering standpoint. The next step in the research should be to validate the proposed model to improve the final product quality. © 2021 Elsevier Inc.
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Kinetic models; Physicochemical characterization of casks; Polyphenols extraction; Tequila maturation; Thermic treatment
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