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RDF description of Development and validation of an analytical method to determine fipronil and its degradation products in soil samples - http://orbis.uaslp.mx/vivo/individual/scopus3082
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date: 2026-08-24T21:51:18
publisher: vivo
type: Document

Bulletin of Environmental Contamination and Toxicology
publication venue for: Development and validation of an analytical method to determine fipronil and its degradation products in soil samples
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Development and validation of an analytical method to determine fipronil and its degradation products in soil samples
related by: authorship_17963
type: Document
most specific type: Article
crisid: 3083
related by: authorship_17964
page start: 744
type: Continuant
type: Information Content Entity
origen: scopus
date time value: article date 3083
freetext keyword: Degradation products; Fipronil; Focused ultrasound probe; GC-ECD Agricultural soils; Analytical method; Degradation products; Fipronil; Focused ultrasound probe; GC-ECD; Limit of detection; Liquid-liquid extraction; Soil sample; Solid-phase extraction; Soxhlet; Gas chromatography; Probes; Ultrasonic applications; Ultrasonics; Degradation; fipronil; insecticide; pyrazole derivative; agriculture; article; chemistry; environmental monitoring; methodology; soil; soil pollutant; validation study; Agriculture; Environmental Monitoring; Insecticides; Pyrazoles; Soil; Soil Pollutants
volume: 89
related by: authorship_17967
chemicalscas: fipronil, 120068-37-3; Insecticides; Pyrazoles; Soil; Soil Pollutants; fipronil, QGH063955F
type: Article
has publication venue: Bulletin of Environmental Contamination and Toxicology
type: Generically Dependent Continuant
type: Entity
abstract: The aim of this study was to develop a methodology for identifying and quantifying Fipronil and its degradation products in soil by gas chromatography-elec-tron capture detector previously extracted using a focused ultrasound probe. This methodology was obtaining a range of recovery between 85 %25 and 120 %25, decreasing approximately solvent used time and cost, respect to other methodologies such as bath ultrasonic, solid-phase extraction, liquid-liquid extraction and soxhlet. The method was validated in fortified matrix, presented linearity in the range of 25-400 μg kg-1, and limit of detection for Fipronil and their products desulfinyl, sulfide and sulfone was 14.7, 9.8, 8.9 and 10.7 μg kg-1, respectively. This process was applied to samples of agricultural soils, where two degradation products desulfinyl and sulfone were found. © Springer Science Business Media, LLC 2012.
most specific type: Document
issue: 4
type: Thing
doi: 10.1007/s00128-012-0780-y
abstract: The aim of this study was to develop a methodology for identifying and quantifying Fipronil and its degradation products in soil by gas chromatography-elec-tron capture detector previously extracted using a focused ultrasound probe. This methodology was obtaining a range of recovery between 85 %25 and 120 %25, decreasing approximately solvent used time and cost, respect to other methodologies such as bath ultrasonic, solid-phase extraction, liquid-liquid extraction and soxhlet. The method was validated in fortified matrix, presented linearity in the range of 25-400 μg kg-1, and limit of detection for Fipronil and their products desulfinyl, sulfide and sulfone was 14.7, 9.8, 8.9 and 10.7 μg kg-1, respectively. This process was applied to samples of agricultural soils, where two degradation products desulfinyl and sulfone were found. © Springer Science%2bBusiness Media, LLC 2012.
page end: 750
related by: authorship_17965
estado: published
related by: authorship_17966
pmid: 22893178
e iscopus: 2-s2.0-84867581860