Preparation of silver nanoparticles-based sensors for the electrochemical detection of thiourea in leaching solutions of waste electrical and electronic equipment
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Waste of electrical and electronic equipment is an interesting secondary resource of base and precious metals. Particularly the use of thiourea-leaching in acidic medium was proposed for noble metals recovery. In this work, a novel and easy-to-use electrochemical sensor was developed, aimed to test thiourea from leaching solutions containing significant thiourea and copper amounts. The sensor was constructed using silver nanoparticles (AgNPs) deposited on screen-printed electrodes. Its performance was studied in a synthetic leaching solution; changes in the overall surface charge of AgNPs resulting in changes in the charge-transfer resistance for the copper ions were evaluated by electrochemical impedance spectroscopy. © 2013 WILEY-VCH Verlag GmbH %26 Co. KGaA, Weinheim.
Waste of electrical and electronic equipment is an interesting secondary resource of base and precious metals. Particularly the use of thiourea-leaching in acidic medium was proposed for noble metals recovery. In this work, a novel and easy-to-use electrochemical sensor was developed, aimed to test thiourea from leaching solutions containing significant thiourea and copper amounts. The sensor was constructed using silver nanoparticles (AgNPs) deposited on screen-printed electrodes. Its performance was studied in a synthetic leaching solution; changes in the overall surface charge of AgNPs resulting in changes in the charge-transfer resistance for the copper ions were evaluated by electrochemical impedance spectroscopy. © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
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Impedance; Nanoparticles; Sensors; Silver; Thiourea
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