Synthesis, spectral and electrochemical characterization of novel 2-(fluoroanilino)-1,4-naphthoquinones
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The preparation of novel 2-(fluoroanilino)-1,4-naphthoquinones is presented. It takes place under mild conditions by reacting the corresponding fluoroaniline and 1,4-naphthoquinone in the presence of a Lewis acid catalyst with strong oxidation properties such as CeCl3·7H 2O. This preparation was also investigated under microwave irradiation. All 1,4-naphthoquinone derivatives were characterized by UV-Vis, IR, 1H and 19F NMR, MS and cyclic voltammetry, to investigate the effect of the fluoro-substituents on their electronic properties. © 2010 Elsevier B.V. All rights reserved.
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2-(Fluoroanilino)-1,4-naphthoquinone; CeCl3·7H2O; Electrochemical oxidation; Lewis acid catalyst; Microwave
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