Structural differences in triosephosphate isomerase from different species and discovery of a multitrypanosomatid inhibitor
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We examined the interfaces of homodimeric triosephosphate isomerase (TIM) from eight different species. The crystal structures of the enzymes showed that a portion of the interface is markedly similar in TIMs from Trypanosoma cruzi (TcTIM), Trypanosoma brucei, and Leishmania mexicana and significantly different from that of TIMs from human, yeast, chicken, Plasmodium falciparum, and Entamoeba histolytica. Since this interfacial region is central in the stability of TcTIM, we hypothesized that it would be possible to find agents that selectively affect the stability of TIMs from the three trypanosomatids. We found that 6,6′-bisbenzothiazole-2,2′ diamine in the low micromolar range causes a desirable irreversible inactivation of the enzymes from the three trypanosomatids and has no effect on the other five TIMs. Thus, the data indicate that it is possible to find compounds that induce selective inactivation of the enzymes from three different trypanosomatids. © 2006 American Chemical Society.
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Biochemistry; Biodiversity; Crystal structure; Enzyme inhibition; Enzymes; Yeast; Homodimeric triosephosphate isomerase (TIM); Micromolar ranges; Trypanosoma cruzi (TcTIM); Trypanosomatids; Enzyme kinetics; 6,6' bisbenzothiazole 2,2' diamine; antitrypanosomal agent; triosephosphate isomerase; unclassified drug; animal cell; animal tissue; article; controlled study; crystal structure; Entamoeba histolytica; enzyme inactivation; enzyme structure; Leishmania; Leishmania mexicana; nonhuman; Plasmodium falciparum; priority journal; protein stability; species differentiation; structure analysis; Trypanosoma; Trypanosoma brucei; Trypanosoma cruzi; Animals; Benzothiazoles; Chickens; Dose-Response Relationship, Drug; Entamoeba histolytica; Enzyme Activation; Fluorescence; Humans; Leishmania mexicana; Species Specificity; Thiazoles; Time Factors; Triose-Phosphate Isomerase; Trypanosoma brucei brucei; Trypanosoma cruzi; Animalia; Entamoeba histolytica; Leishmania mexicana; Plasmodium falciparum; Trypanosoma; Trypanosoma brucei; Trypanosoma cruzi; Trypanosomatidae
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