Photochemistry of fluorophenyl azides in aniline Asymmetric fluoroazobenzenes by N-H singlet nitrene insertion
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Several fluorophenyl azides were photolyzed with aniline at room temperature. Only pentafluoro and 2,6-difluorophenyl azides gave asymmetrical fluoroazobenzenes as the major products. These products were generated by singlet N-H insertion reaction with aniline followed by oxidation of the resulting aromatic hydrazine. © 2004 Elsevier B.V. All rights reserved.
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Fluoroazobenzenes; Fluorophenylazides; Photochemistry; Singlet phenylnitrene aniline; aromatic compound; azide; benzene derivative; fluorine derivative; hydrazine; hydrogen; nitrogen; article; asymmetric synthesis; chemical reaction; controlled study; oxidation; photochemistry; photolysis; room temperature
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