Removal of diethyl phthalate from water solution by adsorption, photo-oxidation, ozonation and advanced oxidation process (UV/H2O2, O3/H2O2 and O3/activated carbon)
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The objective of this work was to compare the effectiveness of conventional technologies (adsorption on activated carbon, AC, and ozonation) and technologies based on advanced oxidation processes, AOPs, (UV/H2O2, O3/AC, O3/H2O2) to remove phthalates from aqueous solution (ultrapure water, surface water and wastewater). Diethyl phthalate (DEP) was chosen as a model pollutant because of its high water solubility (1080mg/L at 293K) and toxicity. The activated carbons showed a high adsorption capacity to adsorb DEP in aqueous solution (up to 858mg/g), besides the adsorption mechanism of DEP on activated carbon is governed by dispersive interactions between π electrons of its aromatic ring with π electrons of the carbon graphene planes. The photodegration process showed that the pH solution does not significantly affect the degradation kinetics of DEP and the first-order kinetic model satisfactorily fitted the experimental data. It was observed that the rate of decomposition of DEP with the O3/H2O2 and O3/AC systems is faster than that with only O3. The technologies based on AOPs (UV/H2O2, O3/H2O2, O3/AC) significantly improve the degradation of DEP compared to conventional technologies (O3, UV). AC adsorption, UV/H2O2, O3/H2O2, and O3/AC showed a high yield to remove DEP; however, the disadvantage of AC adsorption is its much longer time to reach maximum removal. The best system to treat water (ultrapure and natural) polluted with DEP is the O3/AC one since it achieved the highest DEP degradation and TOC removal, as well as the lower water toxicity. © 2012 Elsevier B.V.
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Activated carbon; Adsorption; Diethyl phthalate; Ozonation; Photodegradation Adsorption mechanism; Advanced Oxidation Processes; Aromatic rings; Conventional technology; Degradation kinetics; Diethyl phthalate; Dispersive interactions; First-order kinetic models; Graphene plane; High adsorption capacity; High water; High yield; Phthalates; TOC removal; Ultra-pure water; Water and wastewater; Water solutions; Activated carbon; Degradation; Esters; Graphene; Oxidation resistance; Ozone; Ozone water treatment; Ozonization; Photodegradation; Potassium compounds; Technology; Toxicity; Water pollution; Adsorption; activated carbon; graphene; hydrogen peroxide; ozone; phthalic acid diethyl ester; surface water; ultrapure water; unclassified drug; water; charcoal; oxidizing agent; phthalic acid derivative; phthalic acid diethyl ester; organic carbon; water; activated carbon; adsorption; aqueous solution; photodegradation; photooxidation; phthalate; reaction kinetics; experimental study; removal experiment; solubility; adsorption; advanced oxidation process; aqueous solution; article; controlled study; degradation kinetics; dispersion; electron; intermethod comparison; oxidation; ozonation; pH; photodegradation; photooxidation; priority journal; ultraviolet radiation; waste component removal; waste water; water pollution; adsorption; chemistry; comparative study; isolation and purification; kinetics; methodology; oxidation reduction reaction; radiation exposure; solution and solubility; ultraviolet radiation; water management; water pollutant; chemical interaction; chemical structure; decomposition; mathematical analysis; solubility; total organic carbon; waste component removal; water pollutant; Adsorption; Charcoal; Hydrogen Peroxide; Kinetics; Oxidants; Oxidation-Reduction; Ozone; Phthalic Acids; Solutions; Ultraviolet Rays; Water Pollutants, Chemical; Water Purification
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